JISK0150 : 2020 表面化学分析-亜鉛及び/又はアルミニウム基金属めっきのグロー放電発光分光分析方法

JIS K 0150:2020の規格概要

この規格 K0150は、亜鉛及び/又はアルミニウム基材料からなる金属めっきの厚さ,単位面積当たりの付着量,及び化学組成の定量のためのグロー放電発光分光分析方法について規定。

JISK0150 規格全文情報

規格番号
JIS K0150 
規格名称
表面化学分析-亜鉛及び/又はアルミニウム基金属めっきのグロー放電発光分光分析方法
制定年月日
2009/02/20
最新改正日
2020/07/20
JIS 閲覧
 
対応国際規格

ISO

ISO 16962:2017(IDT)
国際規格分類

ICS

71.040.40
主務大臣
経済産業
JISハンドブック
改訂:履歴
  • 2009-02-20制定日
  • 2013-10-21確認日
  • 2018-10-22確認日
  • 2020-07-20改正日

 

K 0150:2020 (ISO 16962:2017)

 

目 次

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序文 ··································································································································· 1

1 適用範囲························································································································· 1

2 引用規格························································································································· 1

3 用語及び定義 ··················································································································· 2

4 原理······························································································································· 2

5 装置······························································································································· 2

5.1 グロー放電発光分光分析装置 ··························································································· 2

6 グロー放電発光分光分析装置の調整 ····················································································· 4

6.1 概要 ···························································································································· 4

6.2 直流放電源の制御パラメータの設定··················································································· 4

6.3 高周波放電源の制御パラメータの設定················································································ 7

6.4 必要とする装置性能 ······································································································· 9

7 試料の準備とその調製 ······································································································ 10

8 検量線の作成 ·················································································································· 11

8.1 概要 ··························································································································· 11

8.2 検量線作成用試料 ········································································································· 11

8.3 検量線の妥当性確認用試料及び検量線作成用のめっき標準物質 ·············································· 12

8.4 検量線作成用試料のスパッタリング速度の測定 ··································································· 13

8.5 検量線作成用試料の発光強度の測定·················································································· 14

8.6 検量線定数の計算 ········································································································· 14

8.7 標準物質を用いた検量線の妥当性確認··············································································· 14

8.8 検量線の検証及びドリフト補正 ······················································································· 15

9 試験試料の分析 ··············································································································· 16

9.1 放電制御パラメータの調整 ····························································································· 16

9.2 測定時間及びデータ取得速度(サンプリングレート)の設定 ················································· 16

9.3 試験試料の定量深さ方向プロファイルの定量化 ··································································· 16

10 結果の表記 ··················································································································· 16

10.1 定量深さ方向プロファイル ···························································································· 16

10.2 単位面積当たりのめっき付着量の定量 ············································································· 16

10.3 各元素の平均質量分率の決定 ························································································· 17

11 精度 ···························································································································· 18

12 試験報告書 ··················································································································· 18

附属書A(規定)検量線定数の算出及び深さ方向プロファイルの定量化 ········································· 19

附属書B(参考)分析線として使用できるスペクトル線 ······························································ 29

附属書C(参考)単位面積当たりのめっき質量(めっき付着量)の定量 ········································· 30

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K 0150:2020 (ISO 16962:2017)

 

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附属書D(参考)共同実験に関する追加資料 ············································································ 35

参考文献 ···························································································································· 37

 

 

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K 0150:2020 (ISO 16962:2017)

 

まえがき

この規格は,産業標準化法第16条において準用する同法第12条第1項の規定に基づき,一般社団法人

表面化学分析技術国際標準化委員会(JSCA)及び一般財団法人日本規格協会(JSA)から,産業標準原案

を添えて日本産業規格を改正すべきとの申出があり,日本産業標準調査会の審議を経て,経済産業大臣が

改正した日本産業規格である。これによって,JIS K 0150:2009は改正され,この規格に置き換えられた。

この規格は,著作権法で保護対象となっている著作物である。

この規格の一部が,特許権,出願公開後の特許出願又は実用新案権に抵触する可能性があることに注意

を喚起する。経済産業大臣及び日本産業標準調査会は,このような特許権,出願公開後の特許出願及び実

用新案権に関わる確認について,責任はもたない。

 

 

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日本産業規格          JIS

 

K 0150:2020

 

(ISO 16962:2017)

表面化学分析−亜鉛及び/又はアルミニウム基金属めっきのグロー放電発光分光分析方法

Surface chemical analysis-Analysis of zinc- and/or aluminium-basedmetallic coatings by glow-discharge optical-emission spectrometry

序文 

この規格は,2017年に第2版として発行されたISO 16962を基に,技術的内容及び構成を変更すること

なく作成した日本産業規格である。

なお,この規格で点線の下線を施してある参考事項は,対応国際規格にはない事項である。

 

1

適用範囲

この規格は,亜鉛及び/又はアルミニウム基材料からなる金属めっきの厚さ,単位面積当たりの付着量,

及び化学組成の定量のためのグロー放電発光分光分析方法について規定する。合金元素として対象とする

ものは,ニッケル,鉄,けい素,マグネシウム,鉛及びアンチモンである。

この分析方法は,次の質量分率の含有量をもつ元素に適用できる。

− 亜鉛

:質量分率 0.01 %〜100 %

− アルミニウム :質量分率 0.01 %〜100 %

− ニッケル

:質量分率 0.01 %〜20 %

− 鉄

:質量分率 0.01 %〜20 %

− けい素

:質量分率 0.01 %〜15 %

− マグネシウム :質量分率 0.01 %〜20 %

− 鉛

:質量分率 0.005 %〜2 %

− アンチモン

:質量分率 0.005 %〜2 %

注記1 鉛及びアンチモンは,環境汚染及び健康被害の原因となるため最近の素材では添加されない

が,この規格は,これらの元素を含有する古い素材にも適用できる。

注記2 この規格の対応国際規格及びその対応の程度を表す記号を,次に示す。

ISO 16962:2017,Surface chemical analysis−Analysis of zinc- and/or aluminium-based metallic

coatings by glow-discharge optical-emission spectrometry(IDT)

なお,対応の程度を表す記号“IDT”は,ISO/IEC Guide 21-1に基づき,“一致している”

ことを示す。

 

2

引用規格

次に掲げる規格は,この規格に引用されることによって,この規格の規定の一部を構成する。これらの

引用規格は,その最新版(追補を含む。)を適用する。

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JIS K 0150:2020の対応国際規格一覧

  • ISO 16962:2017(IDT)

JIS K 0150:2020の引用国際規格一覧

  • ISO 17925

JIS K 0150:2020の国際規格分類一覧

  • 71.040.40

JIS K 0150:2020の関連規格と引用規格一覧

規格番号
規格名称
G0417
鉄及び鋼-化学成分定量用試料の採取及び調製